8QY9
J22.9-H, fully humanized Fab Fragment based on chimeric J22.9-xi IgG against BCMA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-11-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9184 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 137.360, 55.180, 81.160 |
Unit cell angles | 90.00, 121.02, 90.00 |
Refinement procedure
Resolution | 34.780 - 3.100 |
R-factor | 0.2634 |
Rwork | 0.261 |
R-free | 0.31110 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.443 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.780 | 3.211 |
High resolution limit [Å] | 3.100 | 3.100 |
Number of reflections | 9584 | 942 |
<I/σ(I)> | 6.54 | |
Completeness [%] | 99.2 | 99.37 |
Redundancy | 4.14 | |
CC(1/2) | 0.985 | 0.611 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293.15 | 14% PEG 3350 100 mM BisTris 7.5 mM Cu(II) |