8QN1
OPR3 variant - R283D
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-03-19 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 81.070, 90.780, 111.740 |
Unit cell angles | 90.00, 109.64, 90.00 |
Refinement procedure
Resolution | 46.280 - 1.750 |
R-factor | 0.2359 |
Rwork | 0.235 |
R-free | 0.25420 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.775 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_4761: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.280 | 1.770 |
High resolution limit [Å] | 1.750 | 1.750 |
Number of reflections | 296522 | 4973 |
<I/σ(I)> | 9.3 | |
Completeness [%] | 97.9 | |
Redundancy | 6.9 | |
CC(1/2) | 0.996 | 0.725 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 100 mM Tris-HCl, 50 mM sodium tartate, 8% PEG8000 |