8Q93
Crystal structure of the SARS-COV-2 RBD with neutralizing-VHHs Re30H02 and Re21D01
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-28 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 1 |
Spacegroup name | P 4 3 2 |
Unit cell lengths | 155.615, 155.615, 155.615 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.920 - 3.100 |
R-factor | 0.2033 |
Rwork | 0.200 |
R-free | 0.25720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.771 |
Data reduction software | XDS |
Data scaling software | pointless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.620 | 3.210 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmeas | 0.378 | 3.811 |
Rpim | 0.043 | 0.421 |
Number of reflections | 12249 | 1181 |
<I/σ(I)> | 20.65 | 2.36 |
Completeness [%] | 99.9 | |
Redundancy | 76.9 | |
CC(1/2) | 0.997 | 0.776 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 28% PEG smear broad, 50 mM arginine, 50 mM MSG, 5% Glycerol |