8Q8O
PA14_16140 protein: the regulator of an operon involved in the biofilm formation in PA14 P. aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.649 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 68.862, 68.862, 281.073 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.850 - 2.700 |
R-factor | 0.2162 |
Rwork | 0.210 |
R-free | 0.26880 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 0.575 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.17.1_3660: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.850 | 2.830 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.169 | 1.099 |
Rmeas | 0.173 | 1.126 |
Rpim | 0.037 | 0.243 |
Number of reflections | 11686 | 1478 |
<I/σ(I)> | 22.9 | 5 |
Completeness [%] | 99.7 | 99.3 |
Redundancy | 21.4 | |
CC(1/2) | 0.990 | 0.950 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 292 | 32% PEG 200, 0.2M NaCl, 0.1M acetate pH 4.5 |