8PQN
NQO1 bound to RBS-10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-04-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97918 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 70.748, 178.369, 210.479 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 68.132 - 3.800 |
Rwork | 0.261 |
R-free | 0.36160 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.894 |
Data reduction software | iMOSFLM (7.4.0) |
Data scaling software | pointless (1.12.14) |
Phasing software | PHASER (2.8.3) |
Refinement software | REFMAC (5.8.0405) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 89.180 | 4.010 |
High resolution limit [Å] | 3.800 | 3.800 |
Rmerge | 0.079 | 0.495 |
Number of reflections | 13579 | 1956 |
<I/σ(I)> | 11.4 | 4.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.1 | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.2 | 293 | 300mM TRIS 9.2 2.8M Ammonium Sulfate |