8PNM
Structure of human KCTD15 BTB domain mutant G88D crystal form 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-25 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.976254 |
Spacegroup name | P 1 |
Unit cell lengths | 71.262, 72.091, 94.413 |
Unit cell angles | 89.63, 77.08, 60.50 |
Refinement procedure
Resolution | 61.310 - 1.940 |
R-factor | 0.238 |
Rwork | 0.236 |
R-free | 0.27320 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.090 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 91.330 | 2.120 |
High resolution limit [Å] | 1.940 | 1.960 |
Number of reflections | 75791 | 3791 |
<I/σ(I)> | 14.2 | |
Completeness [%] | 92.5 | |
Redundancy | 3.6 | |
CC(1/2) | 0.999 | 0.594 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 12.5% PEG3350, 0.2M Potassium thiocyanate |