8OU3
Cereblon isoform 4 in complex with novel Benzamide-Type Cereblon Binder 8d
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-08-27 |
Detector | DECTRIS EIGER2 S 16M |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.793, 59.519, 88.149 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.327 - 1.470 |
Rwork | 0.215 |
R-free | 0.23780 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.503 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0405) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.330 | 1.523 |
High resolution limit [Å] | 1.470 | 1.470 |
Number of reflections | 51535 | 8199 |
<I/σ(I)> | 15.28 | 1.09 |
Completeness [%] | 100.0 | |
Redundancy | 12.9 | |
CC(1/2) | 0.999 | 0.664 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 294 | 0.5 M (NH4)H2PO4 |