8OL9
Anti-FIXa Fab in complex with human des-(Gla-EGF1) FIXa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-08-03 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.00000 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 61.440, 97.270, 366.470 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.980 - 2.600 |
R-factor | 0.2695 |
Rwork | 0.267 |
R-free | 0.32330 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.552 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.980 | 2.695 |
High resolution limit [Å] | 2.600 | 2.602 |
Rmerge | 0.132 | 0.806 |
Rmeas | 0.148 | 0.931 |
Rpim | 0.065 | 0.452 |
Number of reflections | 33502 | 2497 |
<I/σ(I)> | 10.62 | 1.28 |
Completeness [%] | 96.2 | 73.6 |
Redundancy | 4.8 | 3.5 |
CC(1/2) | 0.996 | 0.690 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 291 | 0.5 M ammonium sulphate, 0.1 M sodium citrate, pH 5.6, !.0 M lithium sulphate |