8KB8
Structure of the WDR91 WD40 domain complexed with Rab7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-04-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.452, 81.077, 116.404 |
Unit cell angles | 90.00, 94.41, 90.00 |
Refinement procedure
Resolution | 48.490 - 2.490 |
R-factor | 0.2007 |
Rwork | 0.197 |
R-free | 0.26120 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.304 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.490 | 2.590 |
High resolution limit [Å] | 2.490 | 2.490 |
Rmerge | 0.055 | 0.630 |
Number of reflections | 35731 | 3982 |
<I/σ(I)> | 13.5 | |
Completeness [%] | 98.8 | |
Redundancy | 3.5 | |
CC(1/2) | 0.998 | 0.684 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 5% Tacsimate pH 7.0, 0.1 M HEPES pH 7.0, 10% Polyethylene glycol monomethyl ether 5000 |