8II1

Crystal structure of V30M-TTR in complex with BID

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-10-09
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1
Spacegroup name	P 21 21 2
Unit cell lengths	43.066, 85.529, 63.640
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.465 - 1.907
R-factor	0.1963
Rwork	0.195
R-free	0.23060
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.182
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHENIX
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.760	1.980
High resolution limit [Å]	1.907	1.910
Rmeas	0.107	0.704
Number of reflections	18912	1856
<I/σ(I)>	9.4	2.6
Completeness [%]	99.7
Redundancy	5.5
CC(1/2)	0.994	0.834

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG 400, CaCl2, Sodium acetate