8HTA
Solution Structure of the C65A/C167A Mutant of Human Lipocalin-type Prostaglandin D Synthase
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Varian | INOVA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC |
| 10 | 2 | 2 | 3D 1H-13C NOESY aromatic |
| 11 | 2 | 2 | 3D 1H-13C NOESY aliphatic |
| 12 | 2 | 2 | 3D HCCH-TOCSY |
| 13 | 2 | 2 | 2D 1H-13C HSQC |
| 2 | 1 | 1 | 3D CBCA(CO)NH |
| 3 | 1 | 1 | 3D HNCACB |
| 4 | 1 | 1 | 3D 1H-15N NOESY |
| 5 | 1 | 1 | 3D 1H-15N TOCSY |
| 6 | 2 | 2 | 2D 13C-1H (HB)CB(CGCD)HD |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 4 | 1 | 308 |
| 2 | 4 | 1 | 308 |
Conformers
| Conformers Calculated Total Number | 5000 |
| Conformers Submitted Total Number | 10 |
