8HCU
Crystal structure of BCOR/PCGF1/KDM2B complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-12-16 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 67.291, 67.291, 252.035 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 65.010 - 2.200 |
R-factor | 0.20214 |
Rwork | 0.200 |
R-free | 0.23840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5jh5 4hpl |
RMSD bond length | 0.004 |
RMSD bond angle | 1.169 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.4) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0415) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 126.020 | 2.270 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.117 | 1.218 |
Rmeas | 0.122 | 1.262 |
Rpim | 0.033 | 0.329 |
Total number of observations | 421860 | 37997 |
Number of reflections | 30637 | 2605 |
<I/σ(I)> | 12 | 2.4 |
Completeness [%] | 100.0 | |
Redundancy | 13.8 | 14.6 |
CC(1/2) | 0.998 | 0.936 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.2 | 293 | 0.1M magnesium acetate, 0.1M sodium citrate pH6.2, 4% PEG5000MME |