8H45
Blasnase-T13A/P55N
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2021-10-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9791 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 92.656, 92.656, 230.397 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.830 - 1.970 |
Rwork | 0.184 |
R-free | 0.20190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7c8x |
RMSD bond length | 0.012 |
RMSD bond angle | 1.219 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (v1.16) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.950 | 2.010 |
High resolution limit [Å] | 1.970 | 1.970 |
Rpim | 0.033 | 0.636 |
Number of reflections | 71787 | 4561 |
<I/σ(I)> | 17.1 | |
Completeness [%] | 99.9 | |
Redundancy | 25.6 | |
CC(1/2) | 0.999 | 0.431 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | sodium formate |