8H3W
Crystal structure of chicken egg lysozyme at ambient temperature
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU PhotonJet-R |
Temperature [K] | 298 |
Detector technology | PIXEL |
Collection date | 2022-08-30 |
Detector | RIGAKU HyPix-3000 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.030, 79.030, 38.089 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.940 - 2.390 |
R-factor | 0.179 |
Rwork | 0.173 |
R-free | 0.22470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ijv |
Data reduction software | CrysalisPro |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.940 | 2.450 |
High resolution limit [Å] | 2.390 | 2.390 |
Rmerge | 0.688 | 0.584 |
Number of reflections | 5107 | 484 |
<I/σ(I)> | 17.26 | |
Completeness [%] | 100.0 | |
Redundancy | 11.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.09 M HEPES-NaOH pH 7.5, 1.26 M sodium citrate tribasic dihydrate, 10% v/v glycerol |