8GXE
PTPN21 FERM PTP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-01-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 72.313, 228.246, 117.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.840 - 3.000 |
R-factor | 0.2197 |
Rwork | 0.217 |
R-free | 0.26310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bzl |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20rc1_4392) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.840 | 3.107 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.289 | 1.583 |
Rpim | 0.081 | 0.433 |
Number of reflections | 37344 | 2494 |
<I/σ(I)> | 8.89 | |
Completeness [%] | 99.7 | |
Redundancy | 13.3 | |
CC(1/2) | 0.998 | 0.809 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 278 | PEGMME 2000, HEPES pH 7.5 |