8GVV
PTPN21 PTP domain C1108S mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-16 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97915 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 80.382, 56.433, 72.099 |
Unit cell angles | 90.00, 111.90, 90.00 |
Refinement procedure
Resolution | 24.350 - 1.800 |
R-factor | 0.1923 |
Rwork | 0.190 |
R-free | 0.22730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bzl |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20rc1_4392) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.350 | 1.864 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.052 | 0.354 |
Rpim | 0.022 | 0.156 |
Number of reflections | 54178 | 2524 |
<I/σ(I)> | 22.44 | |
Completeness [%] | 99.8 | |
Redundancy | 6.6 | |
CC(1/2) | 0.999 | 0.957 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 278 | PEG 3350, 250 mM Sodium iodide |