8G3U
MBP-Mcl1 in complex with ligand 21
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-01-22 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 99.324, 137.421, 38.563 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 80.500 - 1.940 |
R-factor | 0.19754 |
Rwork | 0.195 |
R-free | 0.23753 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.521 |
Data reduction software | autoPROC (1.1.7) |
Data scaling software | autoPROC (1.1.7) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.500 | 1.977 |
High resolution limit [Å] | 1.940 | 1.943 |
Rmeas | 0.135 | 1.868 |
Rpim | 0.048 | 0.646 |
Number of reflections | 39870 | 1955 |
<I/σ(I)> | 9.3 | 1.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 8 | 8.4 |
CC(1/2) | 0.996 | 0.552 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 285 | 0.11 M Mg Formate, 19.0% (w/v) PEG3350 |