Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-11 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 125.900, 125.900, 55.216 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.510 - 2.920 |
Rwork | 0.246 |
R-free | 0.27960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4x7j |
RMSD bond length | 0.002 |
RMSD bond angle | 1.210 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.510 | 2.970 |
High resolution limit [Å] | 2.920 | 2.920 |
Rmerge | 0.097 | 0.794 |
Number of reflections | 10640 | 510 |
<I/σ(I)> | 9.5 | |
Completeness [%] | 95.3 | |
Redundancy | 6.7 | |
CC(1/2) | 0.997 | 0.817 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 100 mM HEPES pH 7.0, 180 mM Na/K tartrate, 9% PEG3350 |