8EG4
[iU:Ag+:iU] Metal-mediated DNA base pair in a self-assembling rhombohedral lattice
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-18 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.0073 |
Spacegroup name | H 3 |
Unit cell lengths | 106.343, 106.343, 89.835 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.980 - 4.180 |
R-factor | 0.2907 |
Rwork | 0.287 |
R-free | 0.35440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3gbi |
RMSD bond length | 0.005 |
RMSD bond angle | 0.812 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | AutoSol |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 64.307 | 64.307 | 4.662 |
High resolution limit [Å] | 4.180 | 9.982 | 4.181 |
Number of reflections | 3757 | 208 | 207 |
<I/σ(I)> | 12.4 | ||
Completeness [%] | 86.9 | ||
Redundancy | 10.5 | 10.5 | 11 |
CC(1/2) | 0.998 | 0.997 | 0.371 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 100 mM MOPS, 1.25 M magnesium sulfate, 720 uM silver nitrate |