8E5R
Schistosoma mansoni (Blood Fluke) Sulfotransferase/CIDD-0150610 Complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-23 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 140.889, 39.668, 53.839 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 53.840 - 1.400 |
R-factor | 0.17 |
Rwork | 0.169 |
R-free | 0.19910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6bdr |
RMSD bond length | 0.013 |
RMSD bond angle | 1.247 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | PHENIX (1.20_4459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 140.890 | 1.480 |
High resolution limit [Å] | 1.400 | 1.400 |
Rpim | 0.022 | 0.817 |
Number of reflections | 59038 | 8718 |
<I/σ(I)> | 13.3 | 1 |
Completeness [%] | 97.6 | 99.9 |
Redundancy | 6 | 6.2 |
CC(1/2) | 0.999 | 0.515 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | MCSG-3 condition A1: 20% PEG 8000, 0.1 M HEPES:NaOH pH 7.5 |