8DIQ
Tubulin-RB3_SLD-TTL in complex with SB226
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97930 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 105.491, 158.414, 181.226 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.920 - 2.395 |
R-factor | 0.1822 |
Rwork | 0.182 |
R-free | 0.20950 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 6br1 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.505 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.920 | 2.440 |
High resolution limit [Å] | 2.390 | 2.390 |
Rmerge | 0.088 | 0.919 |
Rpim | 0.055 | 0.594 |
Number of reflections | 119484 | 5742 |
<I/σ(I)> | 12.7 | 1.8 |
Completeness [%] | 99.7 | 97.6 |
Redundancy | 6.8 | 6.4 |
CC(1/2) | 0.998 | 0.691 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG4K, MES, Glycerol, CaCl2, MgCl2 |