8DAH
[20 bp edge] Self-Assembled 3D DNA Hexagonal Tensegrity Triangle
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-12 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.00743 |
Spacegroup name | P 63 |
Unit cell lengths | 122.599, 122.599, 57.580 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.130 - 5.470 |
R-factor | 0.1543 |
Rwork | 0.151 |
R-free | 0.19760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7r96 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.906 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.300 | 6.120 |
High resolution limit [Å] | 5.470 | 5.470 |
Number of reflections | 1396 | 203 |
<I/σ(I)> | 10.6 | |
Completeness [%] | 88.5 | |
Redundancy | 13.7 | |
CC(1/2) | 0.998 | 0.482 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.5 | 293 | 1.75 M ammonium sulfate, 120 mM Tris, 120 mM Acetic Acid, 6 mM EDTA |