8D3A
Crystal Structure of DH475 Fab in complex with Man9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-08-03 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.97920 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 126.726, 126.726, 215.816 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 76.940 - 2.900 |
R-factor | 0.2312 |
Rwork | 0.229 |
R-free | 0.27200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5tpp |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.940 | 3.080 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 1.064 | |
Number of reflections | 22928 | 3672 |
<I/σ(I)> | 8 | |
Completeness [%] | 98.0 | 99.1 |
Redundancy | 3.1 | |
CC(1/2) | 0.993 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 1.5 M (NH4)2SO4, 100 mM PIPES, pH 6.0 |