8CT8
Crystal structure of Drosophila melanogaster PRL/CBS-pair domain complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08B1-1 |
Synchrotron site | CLSI |
Beamline | 08B1-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-12-20 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.95374 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 83.311, 83.311, 238.188 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.440 - 2.500 |
R-factor | 0.2285 |
Rwork | 0.225 |
R-free | 0.27500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5k22 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.432 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (1.20_4459) |
Refinement software | PHENIX (1.20_4459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.440 | 2.589 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.042 | 0.284 |
Rmeas | 0.059 | 0.402 |
Rpim | 0.042 | 0.284 |
Number of reflections | 54823 | 5524 |
<I/σ(I)> | 20.04 | 2.19 |
Completeness [%] | 99.7 | 99.52 |
Redundancy | 1.8 | 1.9 |
CC(1/2) | 0.995 | 0.855 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1 M Bis-Tris propane pH 6.5, 17% (wt/vol) PEG3350, 0.2 M NaI |