Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.2 |
| Synchrotron site | BESSY |
| Beamline | 14.2 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2004-01-15 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9537 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 254.246, 246.857, 113.346 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 37.850 - 3.000 |
| R-factor | 0.2595 |
| Rwork | 0.259 |
| R-free | 0.28440 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.009 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | CNS (1.2) |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 3.190 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.104 | |
| Number of reflections | 138965 | 21736 |
| <I/σ(I)> | 12.8 | 2.2 |
| Completeness [%] | 97.9 | 92 |
| Redundancy | 4.8 | |
| CC(1/2) | 0.950 | 0.500 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.7 | 298 | NaCitrate, Hepes, pH 7.7 |
