8BVO
Titin I110-I111 FnIII tandem from the MIR region (I/A5-I/A6)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2015-03-22 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97949 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.287, 46.259, 71.345 |
Unit cell angles | 90.00, 100.73, 90.00 |
Refinement procedure
Resolution | 38.610 - 2.550 |
R-factor | 0.2283 |
Rwork | 0.224 |
R-free | 0.28720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.016 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.610 | 2.600 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmeas | 0.192 | 0.183 |
Number of reflections | 7239 | 401 |
<I/σ(I)> | 6.04 | |
Completeness [%] | 98.9 | |
Redundancy | 3.2 | |
CC(1/2) | 0.982 | 0.424 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 24% (w/v) PEG 1500, 20% (w/v) glycerol |