Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-08-30 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 143.214, 141.199, 87.919 |
| Unit cell angles | 90.00, 124.46, 90.00 |
Refinement procedure
| Resolution | 90.583 - 2.700 |
| Rwork | 0.215 |
| R-free | 0.25410 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | in house model |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.253 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 90.583 | 2.950 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmeas | 0.094 | 0.523 |
| Number of reflections | 39488 | 9173 |
| <I/σ(I)> | 16.8 | 3.58 |
| Completeness [%] | 99.3 | |
| Redundancy | 4.42 | |
| CC(1/2) | 0.998 | 0.882 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | none |
