8BIU
Cystathionine gamma-lyase in complex with cystathionine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-04-10 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9797 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 157.737, 157.737, 93.401 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 93.401 - 1.899 |
R-factor | 0.1632 |
Rwork | 0.152 |
R-free | 0.17830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2nmp |
RMSD bond length | 0.006 |
RMSD bond angle | 0.862 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 93.500 | 1.930 |
High resolution limit [Å] | 1.899 | 1.900 |
Number of reflections | 105469 | 5190 |
<I/σ(I)> | 16 | |
Completeness [%] | 100.0 | |
Redundancy | 19.9 | |
CC(1/2) | 0.992 | 0.461 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 12% (w/v) PEG 3350 0.1M sodium citrate pH 4.6, CYMAL-4 |