Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-07-30 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.97622 |
| Spacegroup name | I 4 |
| Unit cell lengths | 127.675, 127.675, 152.093 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.590 - 1.900 |
| R-factor | 0.1761 |
| Rwork | 0.175 |
| R-free | 0.19860 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1bkd |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.385 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.590 | 2.010 |
| High resolution limit [Å] | 1.895 | 1.900 |
| Number of reflections | 189905 | 30042 |
| <I/σ(I)> | 15.63 | |
| Completeness [%] | 99.6 | |
| Redundancy | 6.9 | |
| CC(1/2) | 0.990 | 0.720 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 14% PEG 1000, Tris 0.1 M pH 7.0 |
