8BAV
Secretagogin (human) in complex with its target peptide from SNAP-25
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 110 |
Detector technology | PIXEL |
Collection date | 2020-05-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97996 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.544, 120.439, 124.066 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.360 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.103 | 0.702 |
Rpim | 0.079 | 0.545 |
Number of reflections | 47592 | 4599 |
<I/σ(I)> | 9.5 | |
Completeness [%] | 99.8 | 99.7 |
Redundancy | 4.5 | 4.6 |
CC(1/2) | 0.996 | 0.601 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 0.2 M Na-acetate 20% PEG3350 |