8A17
Human PTPRM domains FN3-4, in spacegroup P3221
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-17 |
Detector | DECTRIS EIGER2 S 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 87.531, 87.531, 311.235 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 75.800 - 3.090 |
R-factor | 0.2458 |
Rwork | 0.243 |
R-free | 0.28970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v5y |
RMSD bond length | 0.012 |
RMSD bond angle | 1.360 |
Data reduction software | DIALS |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 77.890 | 3.140 |
High resolution limit [Å] | 3.080 | 3.080 |
Number of reflections | 26535 | 1199 |
<I/σ(I)> | 9.1 | |
Completeness [%] | 99.8 | |
Redundancy | 10 | |
CC(1/2) | 0.993 | 0.391 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM ammonium nitrate and 10% PEG 3350 |