8YX9
CD40 in complex with Dacetuzumab Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-05-27 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 199.194, 208.172, 198.061 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.800 - 2.800 |
Rwork | 0.209 |
R-free | 0.26170 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.377 |
Data reduction software | XDS (20220120) |
Data scaling software | Aimless (0.7.7) |
Phasing software | PHASER (2.8.3) |
Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.800 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.151 | 1.350 |
Rpim | 0.042 | 0.375 |
Number of reflections | 101033 | 4996 |
<I/σ(I)> | 17.3 | 2.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.7 | 13.8 |
CC(1/2) | 0.999 | 0.813 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.2 M Ammonium citrate tribasic pH 7.0 20% w/v Polyethylene glycol 3,350 |