8YR7
Crystal structure of human dishevelled 2 (Dvl2) PDZ domain fused with WGEF internal peptide motif
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | RRCAT INDUS-2 BEAMLINE PX-BL21 |
Synchrotron site | RRCAT INDUS-2 |
Beamline | PX-BL21 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2024-02-04 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.978930 |
Spacegroup name | I 41 |
Unit cell lengths | 59.491, 59.491, 58.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.750 - 3.000 |
R-factor | 0.3011 |
Rwork | 0.299 |
R-free | 0.33500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.361 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.070 | 3.190 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.058 | 1.091 |
Number of reflections | 2071 | 336 |
<I/σ(I)> | 27.8 | 2.7 |
Completeness [%] | 99.9 | 100 |
Redundancy | 14.9 | 15.1 |
CC(1/2) | 1.000 | 0.731 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 0.1M Sodium acetate (pH 4.5), 3M Sodium chloride |