8WWR
Crystal structure of apo human dishevelled 2 (Dvl2) PDZ domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-04-27 |
Detector | DECTRIS PILATUS3 X 2M |
Wavelength(s) | 0.87313 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 45.978, 45.978, 78.422 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.510 - 1.750 |
R-factor | 0.2282 |
Rwork | 0.227 |
R-free | 0.25270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.089 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.510 | 1.780 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.067 | 0.731 |
Number of reflections | 9023 | 482 |
<I/σ(I)> | 23.3 | 3.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 17.5 | 15.9 |
CC(1/2) | 0.999 | 0.915 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Tri-sodium citrate, pH 5.6 20% (v/v) Isopropanol 20%(w/v) PEG4000 |