8WHI
Crystal structure of native CLASP2 in complex with CLIP170
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-28 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.987 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.624, 85.545, 114.195 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.312 - 1.853 |
R-factor | 0.1933 |
Rwork | 0.191 |
R-free | 0.23690 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.131 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.880 |
High resolution limit [Å] | 1.850 | 5.020 | 1.850 |
Rmerge | 0.107 | 0.060 | 1.686 |
Rmeas | 0.116 | 0.065 | 1.835 |
Rpim | 0.044 | 0.025 | 0.714 |
Total number of observations | 312929 | ||
Number of reflections | 44523 | 2422 | 2189 |
<I/σ(I)> | 6.4 | ||
Completeness [%] | 100.0 | 99.8 | 99.9 |
Redundancy | 7 | 6.5 | 6.8 |
CC(1/2) | 0.997 | 0.997 | 0.576 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.2 M NaCl, 0.1 M Tris pH 8.5, and 25% w/v PEG 3,350 |