8W0Z
Human LCAD complexed with Lauric Acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-02-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.987 |
Spacegroup name | P 1 |
Unit cell lengths | 86.288, 94.842, 119.163 |
Unit cell angles | 89.24, 74.88, 88.35 |
Refinement procedure
Resolution | 30.120 - 2.000 |
R-factor | 0.214 |
Rwork | 0.214 |
R-free | 0.25600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 10.000 | 2.030 |
High resolution limit [Å] | 2.000 | 5.430 | 2.000 |
Rmerge | 0.080 | 0.049 | 0.506 |
Total number of observations | 604786 | ||
Number of reflections | 243769 | 11600 | 11015 |
<I/σ(I)> | 6.7 | ||
Completeness [%] | 96.1 | 91.3 | 86.8 |
Redundancy | 2.5 | 2.5 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.2 | 291 | TrisHCl, PEG5000MME, NaCl, MgCl2, beta-octyl-b-D-glucoside |