8VKZ
Crystal structure of Glucocorticoid Receptor in complex with an inhibitor
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-12-14 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 38.510, 141.650, 47.900 |
| Unit cell angles | 90.00, 93.46, 90.00 |
Refinement procedure
| Resolution | 70.830 - 2.133 |
| R-factor | 0.19 |
| Rwork | 0.187 |
| R-free | 0.24520 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.900 |
| Data reduction software | autoPROC |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.11.7) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 70.830 | 2.335 |
| High resolution limit [Å] | 2.133 | 2.133 |
| Number of reflections | 16146 | 808 |
| <I/σ(I)> | 8.4 | |
| Completeness [%] | 89.6 | |
| Redundancy | 3.4 | |
| CC(1/2) | 0.998 | 0.533 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 5.5 | 296 | 24% (w/v) PEG 400, 200 mM ammonium acetate, 100 mM sodium citrate pH 5.5 |
