8UCT
Crystal structure of TcPINK1 in complex with PRT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-27 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.987 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 53.216, 53.216, 545.580 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 90.930 - 2.930 |
R-factor | 0.2845 |
Rwork | 0.283 |
R-free | 0.30520 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.776 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.930 | 2.980 |
High resolution limit [Å] | 2.930 | 2.930 |
Rpim | 0.145 | |
Number of reflections | 11014 | 521 |
<I/σ(I)> | 6.1 | 0.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 17.8 | 16.9 |
CC(1/2) | 0.995 | 0.551 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 295 | 100mM HEPES, PEG 4000, 150mM ammonium sulfate |