Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, DESY BEAMLINE P11 |
| Synchrotron site | PETRA III, DESY |
| Beamline | P11 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-05-03 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.033200 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 270.891, 269.263, 185.248 |
| Unit cell angles | 90.00, 131.77, 90.00 |
Refinement procedure
| Resolution | 48.210 - 3.670 |
| R-factor | 0.13817 |
| Rwork | 0.137 |
| R-free | 0.18907 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.722 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.210 | 3.890 |
| High resolution limit [Å] | 3.670 | 3.670 |
| Number of reflections | 105402 | 15220 |
| <I/σ(I)> | 20.64 | 5.8 |
| Completeness [%] | 97.4 | |
| Redundancy | 3.86 | |
| CC(1/2) | 0.999 | 0.955 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.2 M K-Na-tartrate, 100 mM (NH4)2SO4, 100 mM MES pH 6.5 |
