8PWX
PfRH5 bound to monoclonal antibody R5.008
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-08-11 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9999 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 114.990, 114.990, 147.494 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.790 - 3.200 |
R-factor | 0.2429 |
Rwork | 0.240 |
R-free | 0.29350 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.493 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.490 | 3.420 |
High resolution limit [Å] | 3.200 | 3.200 |
Number of reflections | 19138 | 3408 |
<I/σ(I)> | 5.2 | |
Completeness [%] | 100.0 | |
Redundancy | 5.2 | |
CC(1/2) | 0.986 | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.12 M Ethylene Glycol Mix (di-, tri-, tetra- and pentaethylene glycols) 0.1 M Buffer System 3 pH 8.5 (BICINE, Trizma base) 30% v/v Precipitant Mix 3 (glycerol, PEG 4000) |