8P1Q
USP28 in complex with FT206
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-04-09 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.873 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 100.444, 105.541, 178.708 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.090 - 2.790 |
R-factor | 0.2132 |
Rwork | 0.212 |
R-free | 0.23550 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.527 |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.090 | 3.042 |
High resolution limit [Å] | 2.756 | 2.756 |
Number of reflections | 34993 | 2917 |
<I/σ(I)> | 12.8 | |
Completeness [%] | 94.6 | |
Redundancy | 11.9 | |
CC(1/2) | 0.998 | 0.480 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.5 M Na-malonate, pH6.0 0.1M Na-citrate, pH 5.0 |