8DC0
Rat Betaglycan Zona Pellucida Domain (ZPC) in complex with mini monomer TGFb2 (mmTGF-b2-7M2R)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-02-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 76.456, 90.453, 98.872 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.740 - 1.930 |
R-factor | 0.2215 |
Rwork | 0.219 |
R-free | 0.25660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB entries 3QW9 & 5TX4 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.915 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20_4459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.740 | 1.999 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.179 | |
Rmeas | 0.186 | |
Number of reflections | 26131 | 2560 |
<I/σ(I)> | 9.27 | |
Completeness [%] | 99.8 | |
Redundancy | 13 | |
CC(1/2) | 0.997 | 0.404 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 298 | 13% PEG4000, 0.1 M trisodium citrate, 10% ethylene glycol |