7ZOR
Crystal structure of anti-Siglec-15 Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-02-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 127.020, 60.681, 131.258 |
Unit cell angles | 90.00, 107.86, 90.00 |
Refinement procedure
Resolution | 62.467 - 3.933 |
R-factor | 0.2319 |
Rwork | 0.229 |
R-free | 0.27340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5vkk |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 62.467 | 4.001 |
High resolution limit [Å] | 3.933 | 3.933 |
Rmerge | 0.465 | 0.931 |
Rmeas | 0.511 | 1.090 |
Rpim | 0.208 | 0.552 |
Number of reflections | 8960 | 429 |
<I/σ(I)> | 6.4 | 3.2 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 6.1 | 4.4 |
CC(1/2) | 0.865 | 0.511 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 20% (w/v) PEG3350 0.1M HEPES pH7.5 0.2M Magnesium chloride |