7Z27
Crystal structure of the SPOC domain of human RBM15
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-05 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.031, 65.980, 116.808 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.450 - 1.450 |
R-factor | 0.1983 |
Rwork | 0.197 |
R-free | 0.21770 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7z1k |
RMSD bond length | 0.006 |
RMSD bond angle | 0.881 |
Data reduction software | DIALS |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.450 | 1.470 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.112 | 2.080 |
Rmeas | 0.116 | 2.120 |
Number of reflections | 62616 | 4578 |
<I/σ(I)> | 12.9 | |
Completeness [%] | 100.0 | |
Redundancy | 3.5 | |
CC(1/2) | 0.999 | 0.571 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 0.2M Sodium malonate dibasic monohydrate, 0.1M Bis-Tris propane 6.5, 20% w/v PEG 3350 |