7XPM
Ancestral ADH WT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | BRUKER D8 QUEST |
Temperature [K] | 150 |
Detector technology | PIXEL |
Collection date | 2021-12-16 |
Detector | Bruker PHOTON II |
Wavelength(s) | 1.54178 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 113.725, 51.792, 74.220 |
Unit cell angles | 90.00, 128.35, 90.00 |
Refinement procedure
Resolution | 22.300 - 2.350 |
R-factor | 0.2204 |
Rwork | 0.218 |
R-free | 0.26030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5zed |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.360 | 2.440 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.117 | 0.401 |
Number of reflections | 14409 | 1500 |
<I/σ(I)> | 7.1 | |
Completeness [%] | 99.9 | |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 289.2 | PEG 2000, TRIS hydrochloride |