7XE3
Crystal structure of LSD2 in complex with cis-4-Br-2,5-F2-PCPA (S1024)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-16 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.9190 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 143.372, 171.226, 201.918 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.270 - 2.820 |
R-factor | 0.179 |
Rwork | 0.177 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4fwe |
RMSD bond length | 0.007 |
RMSD bond angle | 0.849 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158+SVN) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.270 | 2.890 |
High resolution limit [Å] | 2.820 | 2.820 |
Number of reflections | 60041 | |
<I/σ(I)> | 11.9 | 1.6 |
Completeness [%] | 100.0 | |
Redundancy | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 330mM Ammonium citrate, 26% PEG 3350 |