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7X7Z

The crystal structure of 2+2/4+2 cyclase PloI4

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL19U1
Synchrotron siteSSRF
BeamlineBL19U1
Temperature [K]100
Detector technologyPIXEL
Collection date2016-01-09
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)0.80000
Spacegroup nameP 43 2 2
Unit cell lengths101.659, 101.659, 234.421
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.730 - 2.903
R-factor0.2006
Rwork0.199
R-free0.23340
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5btu
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX (1.14_3260)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.950
High resolution limit [Å]2.9002.900
Rmerge0.2391.373
Number of reflections280331348
<I/σ(I)>12.42.2
Completeness [%]99.9
Redundancy13.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.52890.2 M lithium sulfate, 2.5 M sodium chloride, and 0.1 M sodium acetate/ acetic acid (pH 4.5)

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