7WZC
An open conformation Form2 of switch II for RhoA GDP-bound state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-28 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 31.487, 66.358, 83.363 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.681 - 1.799 |
R-factor | 0.207644606462 |
Rwork | 0.205 |
R-free | 0.26407 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ftn |
RMSD bond length | 0.008 |
RMSD bond angle | 0.892 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.681 | 1.864 |
High resolution limit [Å] | 1.799 | 1.799 |
Rmeas | 0.077 | 0.694 |
Rpim | 0.021 | 0.201 |
Number of reflections | 16632 | 1439 |
<I/σ(I)> | 30.3 | |
Completeness [%] | 99.0 | |
Redundancy | 12.7 | |
CC(1/2) | 0.998 | 0.925 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1M MES, pH6.0, 30% PEG 600, 5% PEG 1000, 10% glycerol |