7WWQ
Crystal structure of human Ufd1-Npl4 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-12-18 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9794 |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 152.958, 165.424, 192.877 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.240 - 2.720 |
R-factor | 0.2426 |
Rwork | 0.241 |
R-free | 0.27690 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.125 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.240 | 2.819 |
High resolution limit [Å] | 2.700 | 2.722 |
Number of reflections | 32527 | 2966 |
<I/σ(I)> | 40.3 | 6.5 |
Completeness [%] | 100.0 | |
Redundancy | 16.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 295 | 0.1M Tris-HCl (pH8.5), 5 % (v/v) glycerol, and 1.3 M magnesium sulfate hydrate |