7VG7
Plexin B1 extracellular fragment in complex with lasso-grafted PB1m6A9 peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-06 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 69.190, 62.490, 82.600 |
Unit cell angles | 90.00, 111.92, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.600 | 2.650 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmeas | 0.473 | |
Number of reflections | 22866 | 3621 |
<I/σ(I)> | 6.43 | |
Completeness [%] | 99.8 | 99.8 |
Redundancy | 19.7 | 18.5 |
CC(1/2) | 0.975 | 0.678 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M MES or HEPES, 14-16% PEG 3350 |